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Wednesday, May 16, 2012

Identification of Fibre | Fiber Identification | Identification of Thermoplastic Fibre


3. To identify the type of sample fibre.
Visual properties:
Colour: White
Handle: Harsh

Physical test:




Preliminary sorting test by heating:
We took small tuft of fibres hold in forceps and brought it slowly up to but not into a small non-luminous flame. Then observe the condition:
















Obs. no.


Behavior


Remark


1


Does not shrink from flame or melt


Non-thermoplastic



For non- thermoplastic fibre:
Bring a small tuft of fibres into a small non-luminous flame –
















Obs. no.


Behavior


Remark


1


Burn with irregular spurting flame, leaving a black inflated, easily powdered residue & emits a smell of burnt hair.


Protein

(Silk & Wool)



Chemical test:












































Obs. no.


Chemical


Behavior


Remark


Cold


Hot


1.


Phenol


Unchanged


Unchanged




2.


Dimethyl formamide


Unchanged


Unchanged




3.


Sulphuric acid


Unchanged


Dissolve


May be silk


4.


Sodium hydroxide


Unchanged


Dissolve


May be wool



Confirmation test:























Obs. no.


Chemical


Behavior


Result


Cold


Hot


1.


Sodium hydroxide


Unchanged


Dissolve


Wool



Visual properties:

Colour: White
Handle: Soft.

Physical test:


Preliminary sorting test by heating:
We took small tuft of fibres hold in forceps and brought it slowly up to but not into a small non-luminous flame. Then observe the condition:



 















Obs. no.


Behavior


Remark


1.


Shrink from flame or melts with the formation of bead


Thermoplastic



For thermoplastic fibre:
Bring a small tuft of fibres into a small non-luminous flame –




















Obs. no.


Behavior


Odor


Residue


Remark


1.


Melts then burns (smoky flame)


Aromatic


Glossy brown bead (not crushable)


May be Polyester



Chemical test:












































Obs. no.


Chemical


Behavior


Remark


Cold


Hot


1.


Sulphuric acid


Unchange


Unchange




2.


Dimethyl formamide


Unchange


Unchange




3.


Phenol


Unchange


Dissolve


May be Polyester


4.


Sodium hydroxide


Unchange


Unchange






Confirmation test:























Obs. no.


Chemical


Behavior


Result


Cold


Hot


1.


Phenol


Unchange


Dissolve


Polyester


 

Conclusion:
I would like to thank our respected teacher for the important instructions. I am also grateful to our lab assistants for their kind help. This experiment helps me to know about the fabric abrasion resistance and its measuring test that is very important for textile testing. I think this will be very helpful in my future life.

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